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Water vapour permeability test and water vapour absorption test are essential for evaluating the performance of materials in various applications. The ISO 17699 and EN ISO 20344 standards provide guidelines for these tests, Ensuring that materials meet the required specifications for moisture management. With the help of advanced testing equipment such as water vapour permeability testers, water vapour absorption testers, and water vapor transmission test equipment, Manufacturers can ensure that their products perform well in real-world conditions. These tests not only enhance material performance but also improve user comfort and product durability, Making them a crucial part of the material evaluation process.
Understanding the interaction between materials and moisture is crucial for many industries, Especially in the manufacturing of textiles and footwear. This is where the Water Vapour Permeability (WVP) Test and Water Vapour Absorption (WVA) Test come into play. These tests are essential for assessing the suitability of materials for their intended use. This article will delve into these tests, focusing on the ISO 17699 standard, the EN ISO 20344 standard, and the related equipment used in these evaluations. By understanding and implementing these tests, Industries can better manage moisture and ensure that their products meet the highest standards of quality and performance.
Water
Vapour Permeability (WVP) is a measure of how well a material allows water
vapor to pass through it. This is a critical property for materials used in
clothing, footwear, and various other applications where moisture management
is essential. The WVP test evaluates how effectively a material can handle
the passage of water vapor, Which can impact comfort, durability, and overall
performance.
Water Vapour
Permeability (WVP)
Water Vapour
Absorption (WVA) refers to the ability of a material to absorb water vapor.
This property is particularly important for materials used in environments
where moisture exposure is frequent. The WVA test helps in understanding how
much moisture a material can hold, Which can affect its performance,
longevity, and user comfort.
Water Vapour
Absorption (WVA)
5.1.1
Unless otherwise specified, cut three samples of dimensions 70 mm x 45 mm.
5.1 Water Vapour
Permeability Test Method
5 Sampling and
Conditioning ISO 17699 EN 13515
5.1.2 For
sheet materials cut test specimens from a range of positions across the full
usable width and length of the sheet material. For a material with a woven
structure this should prevent any two specimens containing the same warp or
weft threads. Prepare test pieces from complete upper assemblies when the
lining material is permanently attached to the upper material
5.1.3 For test
specimens cut from footwear uppers avoid any areas containing seams or
perforations and any other desian features which mean that the test specimen
will not be of uniform thickness across its entire surface area.
Note: It may
not be possible to cut a test specimen of sufficient size from certain types
of footwear, especially children’s and the test specimen size should not be
reduced. lf it is not possible to cut the correct size test specimen from a
shoe upper the materials themselves must be tested.
5.1.4 Mark
each test specimen with a unique reference code.
5.1.5 Store
the cut test specimens in a standard controlled environment specified in EN
12222 for at least 24 h prior to testing and carry out the test in this
atmosphere.
5.1.6 Carry
out 20 000 cycles according to EN 13512
5.2.1 lf the
test is being carried out to assess a single material, then cut two circular
test specimens with a diameter of 45 mm ±5 mm.
5.2
Water Vapour Absorption Test Method
For sheet
materials, cut test specimens from a range of positions across the full
usable width and length of the sheet material. For a material with a woven
structure this should prevent any two specimens containing the same warp or
weft threads.
5.2.2 lf the
test is being carried out to assess a composite assembly of materials used in
a complete product such as a lined shoe, then cut two circular test
specimens, with a diameter as specified in 5.2.1, from each of the materials
used in this assembly.
5.2.3 For test
specimens cut from footwear uppers avoid any areas containing seams or
perforations and any other design features which mean that the test specimen
will not be of uniform thickness across its entire surface area.
Note: It may
not be possible to cut a test specimen of suficient size from certain types
of footwear, especially children’s and the test specimen size should not be
reduced. lf it is not possible to cut the correct size test specimen from a
shoe upper the materials themselves must be tested.
5.2.4 Mark
each test specimen with a reference number
5.2.5 Store
the test specimens in a standard conditioned environment as specified in EN
12222 for at least 24 h before starting the test.
5.2.6 Carry
out 20 000 cycles according to EN 13512.
Equipment
Model
WEW-WVP-WVA-001
WEW-WVP-WVA-002
Internal Dimension(W*D*H)
400×500×500mm(100L)
500×500×600mm(150L)
External Dimension(W*D*H)
900×1075×1400mm
700×1170×1510mm
Internal Material
1.2mm
Thickness SUS#304
Stainless Steel,
Mirror Finished
External Material
1.2mm
Thickness
Cold-rolled Steel
Plate Baking
Temperature Range
-40℃
~ + 150℃
-60℃
~ + 150℃
Temperature Fluctuation
±0.5
℃
±0.5
℃
Temperature Uniformity
≤2℃
≤2℃
Temperature Rate 1
1℃ –
1.5℃/min
1℃ –
1.5℃/min
Temperature Rate 2
3℃ –
3.5℃/min
2.5℃
– 3.5℃/min
Humidity Range
20%~98%RH
20%~98%RH
Humidity Fluctuation
±3%
RH
±3%
RH
Power Voltage
AC 220V ±10%, 50Hz,
60Hz
AC 220V ±10%, 50Hz,
60Hz
Humidity Uniformity
±2%
RH
±2%
RH
Working Positions
6
Positions
6
Positions
Fan Dimension
90x75mm(LxW)
90x75mm(LxW)
The Blade Angel
120
Degrees
120
Degrees
Fan Speed RPM
(1400±100)
rpm.
(1400±100)
rpm.
Water Vapor WVP
Working Positions
6
Postions
6
Postions
Testing Piece
Diameter
φ4.3cm
Diameter
φ4.3cm
Inner test Bottle
3.5
cm
3.5
cm
Metal Container Holds
50
ml
50
ml
WVA Fixture Size
340*210*130mm
340*210*130mm
Water Absorption
A
circular test specimen is clamped across the open end of a test pot
containing a moisture absorbing desiccant.Air of specified humidity and
temperature is blown over the test specimen at a set velocity. The alr within
the pot is circulated by moving the pot which acitates the desiccant. After a
measured time the mass of water vapoul transmited through the test specimen
is determined and the water vapour permeability of the material calculated.
6.1.2.1 Pour
freshly dried silica gel (see 4.1.4) into one of the pots (see 4.1.1) until
it is half full
6.1.2 Procedure
6.1.2.2 Place
a test specimen centrally over the open end of the pot prepared in 6.1.2.1 so
that the surface which would be closer to the source of water vapour in the
final product is uppermost. For example if assessing the perspiration
transmission properties of a footwear upper material, then the surface which
willbe nearer to the foot should be uppermost.
6.1.2.3 Fit a
clamping ring (see 4.1.1.2) centrally over the top of the test specimen and
tighten the ring so that the test specimen is securely held around its edges
and the pot is sealed.
6.1.2.4 Repeat
the procedure in 6.1.2.1 to 6.1.2.3 for the remaining two test specimens.
6.1.2.5 Place
each filed test pot onto the turntable (see 4.1.2.1) and operate the test
machine for 20 h ±4 h. This is to condition the test specimens.
6.1.2.6 Remove
each of the test pots from the turntable.
6.1.2.7 For
each test pot and as quickly as possible remove the clamping ring to release
the test specimen pour away the silica gel from inside the pot, refill the
pot with a similar amount of freshly dried silica gel and replace the test
specimen and clamping ring on the pot by repeating the procedure in 6.1.2.2
and 6.1.2.3
6.1.2.8 With
the minimum of delay use the balance (see 4.1.3) to measure the combined mass
of each test pot, silica gel and test specimen assembly, and record these
values as M, to the nearest 1 mg. Record the time that these measurements
were made as 7o
6.1.2.9
Replace the test pots on the turntable and start the machine.
6.1.2.10 After
11,5 h ±4,5 h stop the test machine and remove the test pots from the
turntable
6.1.2.11 With
the minimum of delay use the balance to measure the combined mass of each of
test pot, silica gel and test specimen assembly, and record these values as
M, to the nearest 1 mg. Also record the time that these measurements were
made as T1.
Either a
single circular test specimen or an assembly of circular test specimens which
is representative of a completed product or taken from a closed shoe upper,
is clamped between an impermeable membrane and the open end of a vertical
cylindrical chamber containing a specified volume of water. After a set time
the mass of water absorbed by the test specimen is measured.
6.2.1 Principle
6.2
Water Vapour Absorption Test Method
6.2.2.1 Use
the balance (see 4.2.2) to measure the mass of each test specimen and record
these values as M0, to the nearest 1 mg.
6.2.2 Procedure
6.2.2.2 lf
assessing an assembly of materials prepare two test specimen stacks as
follows: Place one test specimen of each type of material that is to be
tested together, centrally on top of each other so that the order and
orientation of the specimens in the stack are the same as in the final
oroduct, f possible ioin toaether the test specimens in each stack using a
similar method to that used in manufacture of the actual product. for example
by bonding together with an adhesive layer. The stacks will subsequently be
referred to as test assemblies.
6.2.2.3 Pour
50 cm3 ±5 cm3 of distilled water, temperature according to EN 12222, into
each of the two pots.
6.2.2.4 Place
a test specimen or test assembly centrally over the top of each clamping ring
so that the surface which will be inside the footwear is lowermost.
6.2.2.5 From
this stage onwards take great care to keep the pots vertical and avoid rapid
or jerky movement which might splash water onto the test specimen.
6.2.2.6 Place
a piece of impermeable material (see 4.2.5) centrally over the top of each
test specimen or test assembly.
6.2.2.7 Place
a disk (see 4.2.1.2) centrally over the top of each piece of impermeable
material and clamp the disks to the pots so that the test specimens are
securely held around their edaes and the pot is sealed.
6.2.2.8 Place
the pots in an environment of temperature of according to EN 12222 for 8,0 h
±0,1 h.
6.2.2.9
Quickly dismantle the two test pots taking great care not to splash any of
the water onto the test specimens and use the balance to measure the mass of
each of the test specimens. Record these values as Mf to the nearest 1 mg.
The ISO 17699 standard specifies two test methods to assess the water vapour permeability and water vapour absorption of materials, specifically uppers or complete upper assemblies, regardless of the material type. This standard is crucial for evaluating the suitability of materials in their final applications. The tests are conducted under controlled conditions to ensure accurate and consistent results. The EN ISO 20344 standard, on the other hand, focuses on the testing of personal protective footwear. It includes procedures for evaluating various properties of footwear, including water vapour permeability and absorption. This standard ensures that the footwear provides adequate protection and comfort under different conditions.
4.1.1
The following apparatus and material shall be used: Cylindrical test pots
each with an internal height of 80 mm ±10 mm and internal volume of 100 cm3
±20c3, and including the following:
4.1.1.1 One
circular open end with an internal diameter of D= 30 mm ±1 mm and is known to
the nearest 0,1 mm.
4.1.1.2 A
clamping ring with an internal diameter D.
4.1.1.3 Means
of tightly clamping a test specimen between the clamping ring and the open
end so that the pot is sealed by the test specimen.
4.1.2 Test
machine (see Figure 1)including the following:
4.1.2.1
Vertically mounted turntable which:
a) has at
least three test stations, each of which is capable of holding a test pot so
that its axis is parallel to, and 67 mm ± 2 mm from the axis of rotation of
the turntable;
b) is rotated
at 7,8 rad/s ±0,5 rad/s1)
4.1.2.2 Paddle
type fan which:
a) has three
flat blades inclined at 120° to one another. The blades shall be flat with
approximate dimensions 90 mm x75 mm;
b) is mounted
so that its axle is coaxially aligned with the axis of the turntable (see
4.1.2.1) and the blades pass within a distance of 10 mm ±5 mm of the open
ends of test pots (see 4.1.1) mounted on the turntable;
c) is rotated
at 146 rad/s ±10 rad/s in a direction opposite to the direction of rotation
of the turntable.
Figure 1 – Schematic diagram of apparatus to be used in the water vapour
permeability test
4.1.3
Analytical balance capable of measuring mass up to 200 g to the nearest 1 mg.
4.1.4 Silica
gel with a particle size greater than 2 mm and which is preferably self
indicating.
Freshly dry
the silica gel in a ventilated oven at 125° C ±5 °C for at least 16 h and
cool in a sealed container for at least 6 h. Once dried the silica gel will
remain dry for many days if kept in air tight containers. Typically the
colour of self indicating silica gel will turn from blue when dry to pink or
colourless when saturated.
4.1.5 Press
knife, or similar cutting device, capable of cutting test specimens with a
diameter which is sufficiently larger than D to enable a good seal to be made
around the open end (see 4.1.1.1) of the pot.
4.2.1 Two
round test pots each with a volume of 100 cm3 ±20 cm3 and including the
following.
4.2
Water Vapour Absorption Test Method (see Figure 2)
4.2.1.1 One
open end with a flat annular surface of internal diameter of 35,0 mm ±0,5 mm
and external diameter of at least 20 mm larger. The external diameter can be
provided by a flange of minimum width 10 mm or by a cylinder of minimum wall
thickness 10 mm.
4.2.1.2 A
metal disk of diameter greater than 55 mm.
4.2.1.3 Means
of tightly clamping a test specimen and a piece of impermeable material (see
4.2.5) between the open end and the disk so that the pot is sealed by the
test specimen.
4.2.2
Analytical balance capable of measuring mass up to 100 g to the nearest 1 mg.
4.2.3 Device
capable of measuring time up to 8 h to the nearest 0,1 h, e.g., a stopwatch.
4.2.4
Distilled or deionised water complying with EN ISO 3696.
4.2.5 Two
circular pieces of impermeable material of minimum diameter 55 mm.
4.2.6 Cutting
device such as a press knife, capable of cutting test specimens of diameter
45 mm ±5 mm.
Figure 2 – Apparatus for determination of water vapour absorption
Materials
used in clothing and footwear need to manage moisture effectively to ensure
user comfort and performance. The WVP test helps determine how well a
material can breathe and allow moisture to escape, while the WVA test
evaluates how much moisture the material can absorb. Both tests are essential
for ensuring that the material performs well in real-world conditions.
1. Ensuring
Material Performance
The Importance of
Water Vapour Permeability and Absorption Testing
Materials that
do not manage moisture effectively can deteriorate faster. By conducting WVP
and WVA tests, manufacturers can select materials that offer better
durability and longer service life. This is particularly important in the
footwear industry, where exposure to moisture can lead to premature wear and
tear.
2. Enhancing
Product Durability
Comfort is a
key factor in the success of clothing and footwear. Materials that manage
moisture well help keep the wearer dry and comfortable. The WVP test ensures
that moisture does not build up inside the material, while the WVA test helps
in understanding how much moisture the material can handle before it affects
comfort.
3. Improving User
Comfort**
In the
footwear industry, WVP and WVA tests are used to ensure that materials used
in uppers and linings provide adequate moisture management. This helps in
improving the comfort and durability of footwear.
1. Footwear
Industry**
Applications and
Benefits of WVP and WVA Testing
For textiles,
these tests are crucial in determining how materials will perform in various
environmental conditions. This information helps manufacturers design the products that offer better comfort and longevity.
2. Textile
Industry
In protective
clothing, The effective moisture management is essential for user safety and
comfort. WVP and WVA tests ensure that materials meet the necessary standards
for moisture resistance and absorption.